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e-mail: [zasłonięte]@hirudina.pl
tel. stacjonarny: (032)[zasłonięte]352-04
tel. komórkowy: 513-[zasłonięte]-833
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Adres sklepu:
ul. Księdza Bednorza 14
(pod apteką)
Katowice-Szopienice
Godziny pracy:
Pon - Pt: 8.30 – 16.30
Lokalizacja sklepu:
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Przelew na konto mBank:
16 1140 [zasłonięte] 2[zasłonięte]0040002 [zasłonięte] 406776
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Wszystkie zamówienia realizowane
są przez Pocztę Polską.
Książki wysyłamy zgodnie z
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- po wpłacie na konto
- za pobraniem
Wysyłamy również
za granicę!
Koszty przesyłki są u nas
zawsze zgodne
z aktualnym cennikiem
Poczty Polskiej.
Odbiór osobisty:
Po odbiór książek serdecznie zapraszamy do naszej księgarni w Katowicach-Szopienicach
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WYSYŁKA DZISIAJ !!!
CODZIENNIE W DNI ROBOCZE
WYSTARCZY DO GODZ. 13.00 wysłać do nas:
1) deklarację odbioru przesyłki "za pobraniem"
lub
2) skan przelewu
albo
3) wpłacić za pośrednictwem "Płacę z Allegro"
SYNTEZA PREPARATÓW I ELEMENTY ANALIZY ORGANICZNEJ
pod red. Jerzego Suwińskiego
Stan książki: NOWA
Wydawnictwo Politechniki Ślaskiej 1999
Nakład: 555 egz.
Stron: 266
Okładka: miękka
Spis treści:
Wstęp 5
Ogólne zasady bezpieczeństwa pracy obowiązujące w laboratoriach syntezy organicznej (J. Suwiński) 7
Ogólne sposoby postępowania z odpadami i produktami ubocznymi syntez (J. Suwiński i A. Rajca) 9
Wybór metody otrzymywania preparatu i warunków jego syntezy (A. Skibiński) 14
Spis preparatów 20
4-ACETYLOAMTNO-2-FENYLO-l-OKSY-2//-l,2,3-TRIAZOL.......................................24
2-ACETYLOAMINOTIOFEN..............................................................................................25
(1 -ACETYLO-2-OKSOPROPYLO)(2,4-PENTANODIONIANO)-
(PIRYDYNA)PALLAD(n)....................................................................................................26
(1 - ACETYLO-2-OKSOPROP YLO)(2,4-PENTANODIONlANO)-
(TRIFENYLOFOSFINA)PALLAD(n)..................................................................................26
5-AMINO-l,2-DIMETYLO-4-NITROIMIDAZOL...............................................................27
2-AMINO-7V-FENYLOBENZENOAMIDIMID....................................................................28
3-AiynNO-7//-l,2,4-TRLAZOL.............................................................................................30
4-AMINO-4//-l,2,4-TRIAZOL.............................................................................................31
ANILINA...............................................................................................................................32
BENZAMID...........................................................................................................................34
BENZAMID...........................................................................................................................35
BENZENOSULFINIAN SODU.............................................................................................36
BENZIMIDAZOL..................................................................................................................37
BENZOESAN ETYLU..........................................................................................................38
BENZOESAN FENYLU........................................................................................................39
BENZOFENON.....................................................................................................................40
2-BENZOILOCYKLOHEKSANON.....................................................................................42
BEZWODNIK KWASU 9,10-ETYLENO-9,10-DHYDROANTRACENO-11,12-
DIKARBOKSYLOWEGO.....................................................................................................43
BIS(2,4-PENTANODIONIANO)MIEDŹ(II).........................................................................44
BIS(2,4-PENTANODIONIANO)OKSOWANAD(rV).........................................................45
BIS(2,4-PENTANODIONIANO)PALLAD(II)......................................................................46
p-BROMOANILINA..............................................................................................................47
1-BROMOBUTAN................................................................................................................48
1-BROMOCYKLOHEKSAN................................................................................................49
yV-(4-BROMOFENYLO)ETANOAMID................................................................................50
2-BROMO-l-FENYLOETANON.........................................................................................51
5-BROMO-1-FENYLO-2-METYLO-4-NITROIMIDAZOL................................................52
1-BROMOHEKSAN..............................................................................................................53
4(5)-BROMO-2-METYLO-5(4)-NITROIMIDAZOL...........................................................54
l-BROMO-2-(2-PROPENYLOKSY)BENZEN....................................................................55
(£>i(Z)-l-BROMO-2-(l-PROPENYLOKSY)BENZEN......................................................56
ferf-BUTYLOBENZEN.........................................................................................................57
4-3//-CHTNAZOLON............................................................................................................59
CHLOREK /7-CHLOROBENZOILU....................................................................................59
CHLOREK 3-METOKSYFENYLOMETANOKARBONYLU............................................60
CHLOREK PROPENOŁU...................................................................................................62
p-CHLOROBENZANŁED.............................................,......................................................63
CHLOROCHROMIAN(VI) PIRYDYNIOWY...............'.......................................................64
1-CHLOROMETYLOBENZOTRIAZOL.............................................................................65
2-(4-CHLOROFENYLO)-4-(7VA-DIMETYLOAMINO)CHINAZOLINA..........................67
CHLOROHYDRYDOKARBONYLTRIS(TRff ENYLOFOSFINA)RUTEN(II).................68
l-(l-CHLOROETYLO)BENZOTRIAZOL...........................................................................70
2-CHLORO-2-METYLOBUTAN.........................................................................................71
2-CHLORO-2-METYLOPROPAN.......................................................................................72
2-CHLORO-4(5)-NITROIMIDAZOL...................................................................................73
3-CHLORO-///-l,2,4-TRIAZOL.......................'...................................................................74
CHLOROTRIFENYLOMETAN...........................................................................................75
CHLOROWODOREK (AS)-ALANINIANU METYLU.......................................................76
5(4)-CYJANO-2-METYLO-4(5)-NITROIMIDAZOL..........................................................77
5(4)-CYJANO-4(5)-NITROIMIDAZOL...............................................................................78
4-(l-CYKLOHEKSENYLO)-PERHYDRO-l,4-OKSAZYNA.............................................79
1,3-CYKLOOKTADEEN.......................................................................................................80
CYKLOHEKSANON............................................................................................................81
CYKLOHEKSEN..................................................................................................................82
CYKLOPENTEN...................................................................................................................83
1,2-DBROMOCYKLOHEKSAN.........................................................................................84
3,5-DffiROMO-7i/-l,2,4-TRIAZOL.....................................................................................85
DBUTYLODIJODOCYNA..................................................................................................86
DICHLOROTRIS(TRFENYLOFOSFINA)RUTEN(n).......................................................87
Ll-DIDEUTERO-2-PROPEN-l-OL.....................................................................................88
1,1-DIETOKSY-l-PROPEN..................................................................................................90
2-(Ar,A^-DIETYLOAMINO)-4-(^,iV-DIMETYLOAMINO)-7-NITROCHINAZOLINA.......91
AVV-DIETYLO-3-METOKSYFENYLOETANOAMID.......................................................92
/V,yV-DIETYLO-Af'-(3-NITROFENYLO)MOCZNIK............................................................93
l,4-DETYLO-2>6,7-TRIOKSABICYKLO[2.2.2]OKTAN..................................................94
1,1-DEFENYLOETANOL......................................................................................................95
(£)-l,2-DIFENYLOETEN.....................................................................................................97
4,5-DIFENYLOIMIDAZOL..................................................................................................98
tf./f-DIFENYLOMOCZNIK.................................................................................................99
l,5-DIFENYLO-l,4-PENTADIEN-3-ON...........................................................................100
1,3-DIFENYLO-l-PROPANON..........................................................................................101
2,3;5,6-DI-0-IZOPROPYLIDENO-Z)-MANNO-l,4-LAKTON.........................................102
DIMETOKSYMETAN........................................................................................................104
A^-DIMETYLOCYKLOHEKSYLOAMINA....................................................................105
1.2-DIMETYLO-4-NITROIMIDAZOL...............................................................................107
l,2-DIMETYLO-5-NITROIMIDAZOL...............................................................................108
1,4-DINITROIMIDAZOL....................................................................................................109
2,4(5)-DINITROIMIDAZOL...............................................................................................110
ETANIAN BENZYLU.........................................................................................................111
ETANIAN BUTYLU...........................................................................................................112
ETANIAN BUTYLU...........................................................................................................113
ETANIAN 1-METYLOBUTYLU.......................................................................................114
ETANIAN 3-METYLOBUTYLU.......................................................................................115
ETANIAN 4-METYLOFENYLU........................................................................................116
ETANIAN 1-METYLOPROPYLU.....................................................................................117
ETANIAN 2-METYLOPROPYLU.....................................................................................118
ETANONITRYL..................................................................................................................119
2-ETENYLO-5,5-DIMETYLO-l,3-DIOKSAN..................................................................120
2-ETENYLO-l,3-DIOKSOLAN.........................................................................................121
2-ETENYLO-5-ETYLO-5-HYDROKS YMETYLO- 1,3-DIOKSAN..................................122
iV-(4-ETOKSYFENYLO)ETANOAMID............................................................................124
2-ETYLBDENO-1.3-DIOKSOLAN.....................................................................................125
2-ETYLO-4,7-DIHYDRO-l)3-DIOKSEPINA....................................................................126
2-ETYLO-6,7-DmYDRO-l,3-DIOKSEPINA....................................................................127
l-FENYLO-3-BUTEN-l-OL...............................................................................................128
4-FENYLO-3-BUTEN-2-ON...............................................................................................130
7V-FENYLOETANOAMID..................................................................................................131
1-FENYLOETANON..........................................................................................................132
2-FENYLO-2-HYDROKSYETANIAN METYLU.............................................................134
1-FENYLO-2-METYLO-4-NITROIMIDAZOL.................................................................135
W-FENYLOMOCZNIK........................................................................................................136
l-FENYLO-4-NITROIMIDAZOL........................................................................:..............137
l-FENYLO-4-NITROPIRAZOL.........................................................................................138
2-FENYLO-2-OKSOETANIAN METYLU........................................................................139
5-FENYLO-1-PENTEN-4-YN.............................................................................................141
1-FENYLOPIROL...............................................................................................................142
1-FENYLO-l-PROPANOL.................................................................................................143
5-FENYLO-3.4-TETRAMETYLENOIZOKSAZOL..........................................................145
5-FENYLOTIO-2-NITROANILINA...................................................................................146
3-[y-FENYLO-y-(l,2,4-TRIAZOL-4-ILO)AMIDYNO]-
5-METYLO-l,2,4-OKSADIAZOL......................................................................................148
HYDRAZON CYKLOHEKSANONU................................................................................149
HYDRAZYNO-1,2-DIKARBOKSYDIALDEHYD............................................................150
p-HYDROKSYACETANILID............................................................................................151
4-HYDROKSYBUTANAL.................................................................................................152
1-HYDROKSYMETYLOBENZOTRIAZOL......................................................................153
l-(2-HYDROKSY-5-METYLOFENYLO)ETANON........................................................154
l-IZOPROPYLOAMINO-3-(3-METYLOFENOKSY)-2-PROPANOL.............................156
KWAS2-ACETOKSYBENZENOKARBOKSYLOWY....................................................158
KWAS BENZOESOWY......................................................................................................159
KWAS BENZOESOWY......................................................................................................160
KWAS 2.3-DIBROMO-3-FENYLOPROPANOWY..........................................................163
KWAS 3-FENYLOPROPENOWY.....................................................................................165
KWAS 3-FENYLOPROPENOWY.....................................................................................166
KWAS 3-(4-METYLOFENYLO)PROPENOWY...............................................................167
KWAS(2-METYLO-4-NITROIMIDAZOL-l-ILO)OCTOWY..........................................168
METANIAN 1-METYLOBUTYLU....................................................................................170
METANIAN 1-METYLOPROPYLU..................................................................................170
METANIAN 2-METYLOPROPYLU..................................................................................171
METANIAN 3-METYLOBUTYLU....................................................................................172
METANIAN BUTYLU........................................................................................................173
METOKSYBENZEN...........................................................................................................174
2-METOKSYNAFTALEN..................................................................................................176
l-(4-METOKSYFENYLO)-2-NITROPROPEN.................................................................177
(£)- i (Z)-l,2-METYLENODIOKSY-4-(l-PROPENYLO)BENZEN................'.................177
2-METYLO-2-BUTEN........................................................................................................178
2-METYLO-2-BUTEN........................................................................................................180
2-METYLO-1.4-DINITROIMIDAZOL...............................................................................181
4-METYLOFENOL.......................r....................................................................................182
4-METYLOFENYLOAMINA.............................................................................................184
Ar-(4-METYLOFENYLO)-ETANOAMID..........................................................................185
l-METYLO-6-METOKSY-3-(Af,A^-DIETYLOAMINO)IZOCHINOLINA........................186
l-METYLO-3-NITRO-l,2,4-TRIAZOL..............................................................................187
4-METYLO-3-PENTEN-2-ON............................................................................................188
p-NITROACETANILID......................................................................................................189
3-NITROANILINA..............................................................................................................190
4(5)-NITROIMIDAZOL......................................................................................................192
2-NITROPIRYDYNA..........................................................................................................193
3-NITRO-///-l,2,4-TRIAZOL.............................................................................................194
l-OKSASPIRO[2,5]OKTANO-2-KARBONITRYL...........................................................195
OKSYM l-FENYLO-4-IMEDAZOLIDINONU..................................................................197
PENTA-0-ACETYLO-/J-D-GLUKOPIRANOZA..............................................................198
2-PENTEN...........................................................................................................................199
POLIfDICHLOROC^-l.S-CYKLOOKTADffi^RUTENCII)]...........................................200
l-(2-PROPENYLO)KARBAZOL.......................................................................................201
SÓL 2-METYLO-4(5)-NITROIMIDAZOLU Z 1,8-DIAZABICYKLO[5.4.0]
-7-UNDECENEM................................................................................................................203
SÓL SODOWA ALDEHYDU NITROMALONOWEGO..................................................204
SULFID FENYLOWO-4-NITROFENYLOWY..................................................................205
SULFON FENYLOWO-METYLO WY...............................................................................207
SULFON FENYLOWO-METYLO WY...............................................................................208
TETRA(2-PROPENYLOKSY)SILAN................................................................................210
3-(m-TOLŁOKSY)-l,2-EPOKSYPROPAN.......................................................................211
3-(/?-TOLILOKSY)-l,2-EPOKSYPROPAN.......................................................................212
TRICHLORODEUTEROMETAN......................................................................................214
TRIFENYLOMETANOL....................................................................................................216
//-a>w-TRIKARBONYLBIS(TRIFENYLOFOSFINA)RUTEN(0).......................................218
TRIS(2,4-PENTANODIONlANO)CHROM(ni).................................................................220
TRIS(2,4-PENTANODIONIANO)KOBALT(m)...............................................................221
Syntezy preparatów (S. Krompiec, A. Kudelko, J. Majewski, A. Rajca, A. Skibiński, W. Szczepankiewicz, K. Swierczek, P. Wagner i K. Walczak)
Wprowadzenie do jakościowej analizy organicznej (J. Suwiński) 223
Literatura uzupełniająca 259
Zasady bezpiecznej pracy w laboratorium chemicznym - zalecenia szczegółowe (A. Rajca) 260
ZAPRASZAMY NA INNE NASZE AUKCJE !!!
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